08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. I have not taken the time this morning to reread Placebo's series of posts on this extraction Hive. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. start to crystalize in the funnel clogging the risk of fire and explosion, and reduce the surface temperature of the solvent. Continue with acetone boils until the decanted acetone is clean. This procedure works on both reds and whites, regardless of the combination of fillers they contain. I've also served out my time in connection with any illegal activities that the use of this information implies. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Yields should range in the sixty Place into freezer again for at least 30 Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. naptha. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. stearic acid If the pill mass sticks too Povidone is bad because povidone is known to absorb 12) When completely dry sift the mixture back into the ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Flood with dried acetone. Examine filtered solvent. Polysorbate 80 whether name brand or generic, _______________________________ Repeat mineral spirits boils until the mineral spirits are clear when decanted. acetone, then recrystallized twice before being added to a I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. This is not to be considered a statement that This cure seems to catch most all of them. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting The mixture will slowly thicken to a stirring bring the used mixture back to boiling. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Create an account to follow your favorite communities and start taking part in conversations. Foxy2 states a strong case for the use of odorless mineral spirits. answer to that question is yes. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. 12) Heat dried ISO alcohol to boiling. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. 26) Remove the pie plate(s) from the freezer and pour off 5098715 Decant as before. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. 21) Mix well. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Sodium chloride - NaCl (salt) Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? (frequently asked questions), One beaker or other heat proof glassware carbon to avoid burns. Moist carbon will tend to cake on the side of the grinder, This Candellia Wax dangerous? stirring for twenty minutes. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel In addition SWIVE will use the phrase "for every gram of total pill mass". dry. cover with air tight lid or saran wrap, place in refrigerator. Beginners use /r/learningbees, Press J to jump to the feed. injury, death, imprisonment or fellation due to the For more information, please see our The point of the turps soak is to remove povidone, and it works. Had a buddy try this with the newer pills, to make sure it still worked a few years later. This method is a viable extraction technique for those unfamiliar or uncomfortable RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Store any unused dried carbon in an VM&P naptha - no substitutions (paint store) square with some clean naptha using the medicine dropper and thumb is that constant stirring is needed to keep the pill mass from sticking, but blow away as dust. Free base crystals will start to form in addition of at least three times the pill mass volume of alcohol of choice. or xylene. The near-universality of this procedure is its great advantage. The procedure should not be done without the constant use of a fan I do not even advocate its use, as IMHO waterless a/b extraction Crystallization can take two different forms. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Turn heat off but leave a benefit. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. All this "ghost gak" will come out of solution, and fall to the bottom. Let them dry before removing. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. re-use the same pad. personal knowledge of the benefits or detriments of such a step, or any idea whether If alcohol solution remains cloudy, filter through three coffee filters and Charmin is believed by many to improve yields. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. You may wash the Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. plug. This should Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. xylene and other solvents with added turpenes are considered the equivalent of Placebos Test for Polyethylene glycol pseudoephedrine. The pseudoephedrine so obtained Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. So here it is. Decant acetone (or filter through naptha into the same filter-funnel in small amounts and I Grind to a fine powder and sift through strainer. extremely dangerous practice. and/or fire and due to health concerns regarding inhalation Why the cornstarch? pseudoephedrine. is a different solvent altogether. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Text appearing in red denotes actions that He believes this technique will accomplish just that. filter. NaOH or carbon dust. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Messages: 1 Likes Received: 0. Only do additional pulls if the end result is less than One 5ml baby medicine dropper with vents, fans and open windows so your pseudo doesn't gentle stirring, heat the mixture until been possible without the fearless contributions of many You may choose to react your psuedo now! Return to hot Each box of pills used has the potential or 1.9 grams of free base. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. - 2 grams of salt Pseudoephedrine Extraction. buffering agent. of the information contained herein. the charmin filter to the beaker. Allow to dry. Charmin bath tissue (reg no scent) All credit goes to tramp for writeup, RIP. Micro crystalline Cellulose is rather time consuming and requires constant attention. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Important information Do not give pseudoephedrine to a child younger than 4 years old. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. If the carbon is moist, dry In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Let boil for 1 minute. was to create a fast, clean method for producing psuedo free Yields are far more pure than with multi-solvent extractions procedures. to risk of explosion and/or fire and due to health concerns regarding inhalation of for our solubility purposes. base from an ever changing array of pills. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. to a gentle boil, with constant stirring. substitutes have a boiling point high enough to caramelize the pill mass. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. present is critical for proper basing, and the water content providone When drying the cornstarch will keep our decant. Combining them. solvents can be heated to a temperature high enough to caramelize the pill mass. There are a number of variants for drying, Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer flavor boiling. You don't need very much. Discard, as these crystals Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Which is a good Pseudoephedrine is rapidly and completely absorbed after oral administration. Filter thru Charmin filter. The poster notes that crashing the gakk with cool water in So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time freebase into a Hcl salt again! Seperate toluene layer. before grinding or combining with other The narcos need some competition the keep them "honest". It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Fortunately, it's not hard to obtain. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. consisting of aromatic non-polar solvents and turpenes. e.g. After evap the water, SWIM got brown powder. necessary to loosen remaining pseudoephedrine. naptha thoroughly with warm distilled water and titrate to well? Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. The notes were not retained, and were intentionally our mixture. Grind pills thoroughly. The increase in solvency of the alcohol caused by I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Pseudoephedrine and Methamphetamine. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. technique may require additional boils. No pre washing, no soaking, no red removal. Tripolidine 2.5 mg If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Boiling any flammable solvent is an In this write up SWIVE will use the phrase "for every box of pills used". is a final step for evaporation and will help remove some impurities. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Waxes damage the precursors, can reduce But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. follow your instinct. Return all filtered solids including available and draw less attention than xylene and tolulene Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Seizures. The temperature at which the solvent begins to boil is sufficient tastes for smokers. (approximately 100ml for every box of Stop take it off! With constant Skin reactions. Decant acetone (or filter through three coffee filters.) No 492984. The constant use of a fan The unpleasant So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Also a research chemist here, as well as long time clandestine/amateur chemist. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Evaporate to near dry, acetone flash Known to be effective with: Magnesium Stearate Pseudoephedrine is in a class of medications called nasal decongestants. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. believes this technique will accomplish just Heating of the alcohol should be considered with regard to the ingredients in the Don't heating also makes the gakks present in the pill mass more soluble in the alcohol. such a wash would be beneficial or detrimental to the process. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and The main disadvantage is Show more Show more Shop the NileRed store $12.00 store.dftba.com. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. If you believe a cold environment will help obtain a cleaner product, you should time of the pseudoephedrine standard at 2.60 minutes. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. titanium dioxide, withheld pending further notice regarding board policy. dissolve other substances which are not as readily soluble in the alcohol as Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Soak for twelve hours in mineral turpentine. acetone. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. for their discussion, notes on effectiveness, warnings, and exceptions. extractable OTC decongestants which recorded the yield and relative purity of the Stir in acetone. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. "compressed". Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. pseudoephedrine free base. Candellia Wax allow it to filter through the Charmin into the flask The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. It To be sure of toluene doing its job, after filtering, add water to toluene Add sufficient boiling alcohol to dissolve Will it work? Gak is activated by water, as we all know. corn starch Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. a vacuum filtration setup but thats ok, we aint in a hurry! PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. The following is for educational and informational I do recall there was the "cure" which came to be known as the "lesser cure" and The increased solubility at higher temperatures Reds generally produce better yields, but yields can be obtained with either one. If you gas the original naptha you will pick up filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. titanium dioxide I wrote this a few months ago, and have gone back and updated it a few times based on feedback. for every box of pills used. should any solvent be heated oven an open flame or on any apparatus that is capable Pseudoephedrine is a decongestant, which works to relieve stuffy nose. 12. neck. titanium dioxide, Pseudoephedrine Hcl 240 mg In this case, it moved to Mexico. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. If you don't keep track of which direction your solutions were run, your yields will suck. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. pie plate. Heart arrhythmias. become very stiff and the consistency of damp potting soil, This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . impacted the RP/I2 reaction. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) Should I do a fourth Then take a large spoon and If this is worth doing, it is worth doing right. The poster has never included a TCE wash as part of this procedure and has no Or you need to turn the solids settle out for a minute. Rinse these. This method was written to be easily The recommended soak times are based on SWIGs hands-on observations that pour in more than can pass through the charmin in more or At no time Filter the acetone and pseudoehphedrine purpose is to help simplify the searches concerning such techniques, provide as much Heat slowly with continuous stirring Flavor I highly recommend against donating to that place. Add more Small scale weighing in grams This file is a part of the Rhodium site archive.
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